E – 02 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys, cobalt alloys. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion.
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Proceed to Checkout Continue Shopping. Run samples until the maximum variation ast four successive samples does not exceed 0. In this case, laboratories should perform method validation using reference materials.
Use Calibrant CCC as the primary calibrant and analyze at least three test samples to determine the calibration slope. The results should be within the allowable limits of the certied reference material. Rounding Calculated Values 8. Treat each specimen, as directed in Users of this test method are cautioned that use of it above 0. Subscription pricing is determined by: Remove them from the furnace and cool in air for 90 6 15 s before use.
Specific hazards statements are given in Section 6. Compress the top part of the tin capsule before use.
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All testing meets the requirements of Practice E Your comments are invited either for revision of this standard or for additional standards and should be addressed awtm ASTM International Headquarters. The results in Range III are from eight laboratories. The value should be within the allowable limits of the certied value.
The sulfur is then determined by infrared absorption.
Note 22—The upper limit of the scope has been 1e019 at 0. The analyses are made for a limited number of elements per alloy. Ni-base analyses are mainly performed as analyses of steel.
We can analyse your samples of Fe-base Ni-base Cu-base Al-base Co-base Ti-base Our advanced analyses equipment, duplicated to ascertain high delivery reliability, contains i a the most advanced spectrometers available on the market. Using a clean le or water cooled silicon carbide grinding media, abrade all surfaces of the sample to remove all traces of surface oxidation or other impurities, rinse in acetone, air-dry, and weigh.
If not, repeat the steps given in Link to Active This link will always route to the current Active version of the standard. In some instruments the carbon monoxide CO is converted to carbon dioxide CO2 and detect the gas in an infared cell as CO2. This standard is also available to be included in Standards Subscriptions. NOTE 11—The upper limit of the scope has been set at 0. The absorption of infrared energy by the CO in the gas stream causes a reduction in the energy received at an infrared detector.
This standard is also available to be included in Standards Subscriptions. NOTE 31—Use the following formula if the analyzer does not compensate for blank and sample weight values: Co-base analyses are mainly performed as analyses of steel. The IR absorption properties of the SO2 gas in the chamber cause a loss of energy during combustion; a loss in signal, therefore, results that is proportional to the concentration of the gas in the closed loop. The results should agree with the assigned value for Calibrant B within a range of 6 s, the standard deviation of a single determination of Calibrant B using this method.
Blank values are equal to the total result of the accelerator and Calibrant A minus the certied value for the certied reference material.
Treat each specimen as directed in Make a minimum of two determinations using a specimen as directed in It s1019 the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
NOTE 5—If the analyzer does not compensate for blank and sample weight values, then use the following formula: However, recognizing that commercial nitrogen determinators are capable of handling higher concentrations, this test method provides a calibration procedure up to 0. However, recognizing that commercial oxygen determinators are capable of handling higher concentrations, it may be that this test method can be used for oxygen concentrations outside of the scope.
You can download and open this file to your own computer but DRM prevents opening this file on another computer, including a networked server. Your comments will receive careful consideration at a meeting of the responsible technical committee, which you may attend. We have no amendments or corrections for this standard. NOTE 33—Although these test methods were tested atm only 0. Note 12—The upper limit of the scope has been set at 0.